da Dillali China 2-Amino-5-chlorobenzophenone Mai Samar da Kayan masana'antu da Mai ba da kayayyaki |LonGoChem
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Kayayyaki

2-Amino-5-chlorobenzophenone

Takaitaccen Bayani:

Sunan samfurin: 2-Amino-5-chlorobenzophenone
Lambar CAS: 719-59-5
Lambar shiga EINECS: 211-949-7
Tsarin kwayoyin halitta: C13H10ClNO
Nauyin Kwayoyin: 231.68


Cikakken Bayani

Tags samfurin

Tsarin Tsari

5
Na zahiri

Bayyanar: Yellow crystalline foda
Girma: 1.33
Matsayin narkewa: 96-98 ° C (lit.)
Tushen tafasa: 207 ° C
Refractivity: 1.6000 (kimanta)
Wutar walƙiya: 211 ° C

Bayanan Tsaro
Gabaɗaya

Aikace-aikace
Metabolite na Diazepam;yana da tasirin anticonvulsant mai rauni sosai.

Matsakaicin magunguna.Kera magunguna irin su Librium da Valium.
Tasirin muhalli
Yana da ɗan haɗari ga ruwa, kar a ƙyale wanda ba shi da ruwa ko babba ya haɗu da ruwan ƙasa, hanyoyin ruwa ko najasa, kuma kar a fitar da kayan cikin muhallin da ke kewaye ba tare da izinin gwamnati ba.

Kayayyaki da Kwanciyar hankali
Barga a yanayin zafi da matsa lamba, kauce wa lamba tare da oxides

Hanyoyin ajiya
Ajiye akwati sosai kuma a adana a wuri mai sanyi, busasshiyar wuri a cikin akwati mai ɗimbin yawa.

Hanyar hadawa
(1) Samuwar ta hanyar amsawar p-chloroaniline tare da benzoyl chloride.Ƙara p-chlorobenzene a cikin tukunyar gilashin da aka yi da gilashi a 70 ° C ko ƙasa, sa a cikin zinc chloride mai anhydrous, ƙara benzoyl chloride dropwise tare da motsawa, sa'an nan kuma tada zazzabi, riƙe a 195-205 ° C na 2h, wanke sau biyar tare da ruwan zafi a 90-95 ° C (ruwan ruwa da maganin wankewa sun dawo da benzoic acid da zinc chloride) a kimanin 100 ° C, ƙara sulfuric acid sannu a hankali, riƙe a 142 ° C na 40min.Daskararrun suna haɗe cikin ruwa.A ƙarƙashin motsawa, ana daidaita pH tare da alkali mai ruwa zuwa ƙasa da 1 kuma an tace shi a 20-25 ° C.An dawo da tacewa azaman p-chloroaniline.Ana gauraya kek ɗin tacewa kuma a dakatar da shi a cikin ruwa, ba tare da bata lokaci ba zuwa pH = 6, an tace bushe, wanke da ruwa zuwa tsaka tsaki kuma a bushe don samun ɗanyen samfurin.Sa'an nan kuma ƙara 6-7 sau ethanol, 6% carbon kunnawa, reflux na 30min, tace da crystallize, bushe don samun samfurin mai kyau.(2) p-Nitrochlorobenzene da haɗin zoben cyanobenzyl don samun isoxazole, sannan buɗe zobe, raguwa don samun.


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